| Table 9:
73Ge NMR spectral data for linear oligogermanesa, b. |
| | Compound | 73Ge (ppm) | (Hz) | Reference |
| | Ge2H6 (25) | −312 | 13 | [10] | | | | | | | Ge3H8 (26) | −298 | 25 |
[10] | | −310 | 40 | | | | | | | Ge4H10 (27) | −284 | 76 |
[10] | | −300 | 100 | | | | | | | MeH2GeGeH3 (28) | −306 | 2 |
[10] | | −210 | 13 | | MeH2GeGeH2Me (29) | −209 | 7 | [10] | | | | | | | Me2HGeGeH3 (30) | −296 | 7 |
[10] | | −127 | 3 | | | | | | | Me3GeGeH3 (31) | −296 | 13 |
[10] | | −48 | 63 | | | | | | | MeH2GeGe(MeH)GeH2Me (32) | −206 | 2 |
[10] | | −125 | 8 | | | | | | | Me2ClGeGeH3 (33) | −281 | 39 | [11] | | Ge2Me6 (34) | −59 | n/r | [11] | | Ge2Et6 (35) | −35 | n/r | [12] | | Ge2Ph6 (36) | −67 | 90 | [11] | | Et3GeGePh3 (37) | −64 | 270 | [13] | | | | | | | GeGePh3 (38) | −56 | 80 |
[13] | | −65 | 240 | | | | | | | GeGePh3 (39) | −58 | 100 |
[13] | | −65 | 340 | | GeGePh3 (40) | −52 | 30 | [13] | | PhMe2GeGePh3 (41) | −65 | 90 | [13] | | | | | | | Ph3GeGeL (42) | −57 | 90 |
[13] | | −64 | 330 | | | | | | | Ph3GeGeGeL (43) | −57 | 310 |
[13] | | −63 | 310 | | | | | | | Ph3GeGeGePh2L (44) | −54 | 120 |
[13] | | −65 | 390 | | | | | | | LGeGePh2GeL (45) | −111 | 180 | [13] | | LPh2GeGePh2GePh2L (46) | −121 | 170 | [13] |
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aData are referenced to Me4Ge.
bL: CH2CH2OEt.
|