Research Article
Critical Analysis on the Structural and Magnetic Properties of Bulk and Nanocrystalline Cu-Fe-O
Table 1
Peak position, intensity, and hkl values of possible secondary phases in Fe-doped CuO from XRD pattern.
| CuO | CuFe2O4 | Fe3O4 | Fe2O3 |
| 2θ | Int | 2θ | Int | hkl | 2θ | Int | hkl | 2θ | Int |
| 35.663 | 999 | 35.543 | 999 | 311 | 35.443 | 999 | 3 1 1 | 35.631 | 719 | 46.401 | 14 | 47.299 | 009 | 331 | 47.162 | 007 | 3 3 1 | — | — | 53.615 | 71 | 53.596 | 076 | 422 | 53.438 | 088 | 4 2 2 | 54.066 | 427 | 56.863 | 06 | 57.135 | 259 | 511 | 56.964 | 281 | 5 1 1 | — | — | 65.989 | 96 | 65.974 | 010 | 531 | 65.770 | 009 | 5 3 1 | 66.030 | 003 | 75.235 | 35 | 75.244 | 027 | 622 | 75.002 | 030 | 6 2 2 | 75.456 | 059 | 87.103 | 09 | 87.051 | 022 | 642 | 86.754 | 030 | 6 4 2 | — | — | 90.064 | 15 | 89.964 | 081 | 731 | 89.650 | 102 | 7 3 1 | — | — |
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