Research Article
Kinetic Studies of Atom Transfer Radical Polymerisations of Styrene and Chloromethylstyrene with Poly(3-hexyl thiophene) Macroinitiator
Table 1
Recipes for carrying out ATRP for styrene and chloromethylstyrene with the use of P3HT macroinitiator.
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Styrene = 1.7 mL, chloromethylstyrene = 2.13 mL, P3HT = 1 g, Cu(II)Br2 = 0.223 g, PMDEA = 0.02 mL, (i) Sn(EH)2 = 0.00648 mL for the AGET-ATRP system. (ii) AIBN = 0.003 mL for the SR&NI-ATRP system. (iii) Cu(I)Br = 0.14 mL for the normal ATRP system. |