Synthesis, X-Ray Structure, and Characterization of Catena-bis(benzoate)bis{N,N-bis(2-hydroxyethyl)glycinate}cadmium(II)

Table 2

Selected bond lengths (Å) and angles (^∘) for complex 1 a.

Cd(1)-O(1)	2.373(2)	Cd(2)-O(11)	2.190(3)
Cd(1)-O(3)	2.375(3)	C(1)^b-O(1)	1.242(5)
Cd(1)-O(4)	2.557(3)	C(1)^b-O(2)	1.253(5)
Cd(1)-N(1)	2.465(3)	C(11)^c-O(11)	1.264(5)
Cd(2)-O(1)	2.550(2)	C(11)^c-O(12)	1.234(5)
Cd(2)-O(2)	2.311(4)
O(1)-Cd(1)-O(1^′)	153.4(1)	O(1)-Cd(2)-O(1^′′)	156.8(1)
O(1)-Cd(1)-N(1^′)	119.8(1)	O(1)-Cd(2)-O(2)	52.9(1)
O(3)-Cd(1)-O(3^′)	87.7(2)	O(2)-Cd(2)-O(2^′′)	94.2(2)
O(3)-Cd(1)-O(4^′)	155.3(1)	O(2)-Cd(2)-O(11)	129.6(1)
O(4)-Cd(1)-O(4^′)	75.3(2)	O(11)-Cd(2)-O(11^′′)	117.6(2)
O(4)-Cd(1)-N(1^′)	84.8(1)	O(11)-Cd(2)-O(2^′′)	93.1(1)
N(1)-Cd(1)-N(1^′)	147.5(2)	O(1)-C(1)^b-O(2)	121.2(4)
N(1)-Cd(1)-O(4)	69.3(1)	O(11)-C(11)^c-O(12)	123.0(4)

aSymmetry transformations used to generate equivalent atoms:(′) 𝑦, 𝑥, −𝑧; (′′) −𝑦+1, −𝑧+1, −𝑧+1/2.
bThis carbon atom (not labeled in Figure 1) belongs to the carboxylate group of the bicinate(−1) ligand.
cThis carbon atom (not labeled in Figure 1) belongs to the carboxylate group of the benzoate ligand.