A Synthetic Approach of New Trans-Substituted Hydroxylporphyrins

Table 2

Crystallographic data for 4  2H₂O.

	4 2H2O
Formula	C52H50N4O4
Fw	794.96
Space group	P21/n
a ()	17.288(4)
b ()	8.2587(17)
𝑐 ()	17.829(4)
𝛼 (°)	90
𝛽 (°)	106.15(3)
𝛾 (°)	90
V (Å^3)	2445.1(9)
Z	2
T (°C)	25
Radiation	Mo K𝛼
𝜚calcd(gcm^−3)	1.080
𝜇(mm^−1)	0.069
Reflections with 𝐼>2𝜎(𝐼)	2338
𝑅^a1	0.0723
𝑤𝑅^a2	0.1890

^a𝑤=1/[𝜎²(𝐹^2𝑜)+(𝛼𝑃)²+𝑏𝑃]and𝑃=[max(𝐹^2𝑜,0)+2𝐹^2𝑐]/3.