Research Article

Stability-Indicating HPTLC Method for Determination of Duloxetine Hydrochloride in Bulk Drug and Tablet Formulation

Table 5

Summary of validation parameters.

ParameterData

Linearity range600–2000 (ng per spot)
Limit of detection100 (ng per spot)
Limit of quantification350 (ng per spot)
Correlation coefficient 0 . 9 9 6 2 ± 0 . 0 0 1 5
Recovery (%) 9 9 . 8 5 ± 0 . 6 0
Precision (%RSD)
Interday0.35
Intraday0.33