Quantitative Analysis of Volatile Impurities in Diallyldimethylammonium Chloride Monomer Solution by Gas Chromatography Coupled with Liquid-Liquid Extraction

Table 3

Precision and recovery for allyl chloride and its derivatives ().

Impurities	Initial found (mg L^−1)	Added (mg L^−1)	Total found (mg L^−1)	Recovery (%)	RSD (%)
Dimethylamine	10.75	10.0	22.30	107.5	5.95
	19.12	20.0	37.39	95.6	3.77
	27.42	30.0	56.21	97.9	1.67
Allyldimethylamine	24.85	25.0	49.55	99.4	1.59
	32.44	30.0	64.68	103.6	1.74
	41.59	40.0	84.93	104.1	2.49
Allyl chloride	12.39	10.0	22.23	99.3	1.62
	19.00	20.0	37.05	95.0	1.45
	26.80	30.0	58.67	103.3	2.21
Allyl alcohol	11.71	10.0	21.47	98.9	2.15
	16.24	20.0	34.64	95.6	3.75
	24.73	30.0	53.42	97.6	1.97
Allyl aldehyde	24.88	10.0	33.97	97.4	1.40
	38.77	20.0	56.95	96.9	2.05
	53.58	30.0	83.16	99.5	1.73