International Journal of Photoenergy 
Volume 2008 (2008), Article ID 245981, 4 pages
doi:10.1155/2008/245981
Research Article

Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles

M. Rashidzadeh

Catalysis Research Center, Research Institute of Petroleum Industry, P.O. Box 14665-1998, Tehran 1485733111, Iran

Received 7 April 2008; Accepted 11 August 2008

Recommended by J. Yu

Abstract

Nanosized crystals of anatase phase TiO2 with high-thermal stability was synthesized in the range of 15–17 nm via sol-gel method using titanium n-butoxide precursor. Synthesize was done at two different temperatures, that is, 200 and 300C and the final products were calcined at 400C. The final products were characterized by N2 adsorption, X-ray diffraction, FT-IR, and TEM and tested in a photoreactor using fluorescien as model molecule. For thermal stability investigation, the sample prepared at 300C was heated up to 800, 850, and 900C, the XRD results showed that the synthesized anatase phase was stable up to 850C. Photocatalytic activity of the prepared samples showed that the fluorescien degradation followed a pseudo-first-order kinetic.