Research Article
Poly(delta-gluconolactone) and Poly(delta-gluconolactone-ε-caprolactone) from delta-Gluconolactone and ε-Caprolactone by Ring-Opening Polymerization
Table 2
ROP of d-GL with various time and temperature in MBTO catalytic .
| ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
reactions were performed in n-octane with MBTO, [d-GL]/[Cat] = 500 : 1, monomer : initiator = 1000 : 1. by integration of methane resonances in 1H NMR of PGL (DMSO-d6, 600 MHz). |