Research Article
Titrimetric and Spectrophotometric Assay of Ganciclovir in Pharmaceuticals Using Cerium(IV) Sulphate as the Oxidimetric Agent
Table 3
Evaluation of intraday and interday accuracy and precision.
|
Method* |
GNC taken | Intraday accuracy and precision | Interday accuracy and precision | GNC found | %RE | %RSD | GNC found | %RE | %RSD |
| Titrimetry |
3.0 | 3.03 | 1.00 | 1.27 | 2.96 | 1.26 | 2.34 |
6.0 | 6.04 | 0.67 | 0.81 | 1.08 | 1.08 | 1.47 |
9.0 | 9.02 | 0.22 | 0.66 | 8.94 | 0.66 | 1.62 |
| Spectrophotometry |
2.0 | 2.04 | 2.00 | 3.10 | 2.05 | 2.5 | 3.26 |
4.0 | 4.04 | 1.00 | 1.13 | 4.08 | 2.0 | 1.56 |
6.0 | 5.83 | 2.83 | 0.50 | 5.90 | 1.67 | 2.13 |
|
|
RE: relative error; RSD: relative standard deviation.
*In titrimetry, GNCs taken/found are in mg and they are μg mL−1 in spectrophotometry.
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