Research Article

Quality by Design Approach for the Development and Validation of Glipizide, an Antidiabetic Drug, by RP-UPLC with Application to Formulated Forms and Urine

Table 8

Results of determination of GPZ in spiked urine sample.

Spiked concentration µg mL−1Founda  ± SD % Recovery ± RSDb

150.23155.46 ± 3.16103.48 ± 1.01
200.22209.24 ± 1.28104.51 ± 1.02
250.32258.12 ± 2.45103.12 ± 0.98

aMean value of five determinations.
bRSD is relative standard deviation.