Acylation of Chiral Alcohols: A Simple Procedure for Chiral GC Analysis

Table 3

Effect of the temperature on the synthesis of 1-methylhexyl acetate. Reaction conditions: 1 : 1 molar ratio acetic acid : alcohol, 24 h and no solvent.

Entry	Temperature (°C)	% 1-methylhexyl acetate	SD	Tukey-Kramer*
1	100	71.24	2.15	A
2	120	64.13	1.11	B
3	140	66.41	2.56	B

*Tukey-Kramer pairwise differences adjustment method, =3.