Table 4: Separation factor values (α) of the enantiomers of some acyclic alcohols and their corresponding acetyl derivatives.

EntryT (°C)AlcoholαACα
RTRT
(−)(+)(−)(+)

1452949.table.004a401.831.931.052.944.241.44a
2452949.table.004b405.105.451.073.7911.313.00a
3452949.table.004c507.618.021.056.3512.391.95b
4452949.table.004d506.797.381.091.351.371.02a
5452949.table.004e801.921.921.002.321.761.32b
6452949.table.004f506.916.911.009.049.041.00c
7452949.table.004g805.365.451.025.047.461.50c
8452949.table.004h7010.1810.181.007.539.911.32c

T: oven GC temperature (°C); RT: retention time; α: separation factor; AC: acetyl derivatives; the elution order of the acetylated enantiomers was assumed from the literature [34, 35]; a: 1H and 13C NMR spectral data were in agreement with those published in [37]; b: 1H and 13C NMR spectral data were in agreement with those published in [38]; c: 1H and 13C NMR spectral data in the appendix.