| Formula: [(C3H7)4N]2Hg2Cl6 | = 986.6 | Color/shape | Colorless/prismatic | Crystal dimensions | 0.22 0.18 0.11 mm | Crystal system | Monoclinic | Space group | C 2/ (N° 15) | Å, Å, | = 7409.0(7) Å3 | Å, β =91.686 | = 8, = 8.726 mm−1 | Temperature (K) | 173 | Radiation, λ (Å), monochromator |
Mo, 0.71069, graphite | Scan angle (°) | θ-θ | θ Range (°) | 1.4–30 | Range of , , | −26→27, −16→18, −40→40 | Reflections collected/unique | 42266/10658 ( = 0.047) | Observed reflections [Fo > 2σ(Fo)] | 8486 | Absorption correction | Multiscan (SADABS) | , | 0.542, 0.823 | Structure resolution | Paterson methods: SHELXS-86 | Structure refinement with | SHELXL-97 | Refinement | full matrix | Refined parameters | 348 | Goodness of fit | 1.177 | Final and Rw | 0.038, 0.087 | Final and Rw (for all data) | 0.057, 0.097 | Largest feature diff. map | 1.565, −1.354 e−/Å3 | = 1/[ σ 2(Fo)2 + (0.035 )2 + ] | = [Fo2 + 2Fc2]/3 |
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