Research Article
An Efficient and Mild Method for the Synthesis and Hydrazinolysis of N-Glyoxylamino Acid Esters
Table 1
Yield %, Mp (°C) and Elemental Analysis of 10a–d and 11a–d.
| Cpd no. | Yield (%) | Mp (°C) | Elemental analysis calcd (found) | C | H | N |
| 10a | 89 | 108–110 | 57.53 (57.85) | 5.52 (5.81) | 9.58 (9.33) | 10b | 87 | 90–92 | 57.53 (57.28) | 5.52 (5.81) | 9.58 (9.33) | 10c | 90 | 100–102 | 58.82 (59.03) | 5.92 (5.81) | 9.15 (8.89) | 10d | 92 | 92–94 | 61.07 (61.23) | 6.63 (6.79) | 8.38 (8.57) | 11a | 80 | 198–200 | 54.54 (54.88) | 6.10 (6.43) | 21.20 (21.50) | 11b | 86 | 204–206 | 56.10 (55.87) | 6.52 (6.81) | 20.13 (19.89) | 11c | 84 | 195–197 | 57.52 (57.33) | 6.90 (7.11) | 19.17 (19.42) | 11d | 90 | 186–188 | 59.98 (60.11) | 7.55 (7.67) | 17.49 (17.68) |
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