Research Article

An Efficient and Mild Method for the Synthesis and Hydrazinolysis of N-Glyoxylamino Acid Esters

Table 1

Yield %, Mp (°C) and Elemental Analysis of 10ad and 11ad.

Cpd no.Yield (%)Mp (°C)Elemental analysis calcd (found)
CHN

10a 89108–11057.53 (57.85)5.52 (5.81)9.58 (9.33)
10b 8790–9257.53 (57.28)5.52 (5.81)9.58 (9.33)
10c 90100–10258.82 (59.03)5.92 (5.81)9.15 (8.89)
10d9292–9461.07 (61.23)6.63 (6.79)8.38 (8.57)
11a80198–20054.54 (54.88)6.10 (6.43)21.20 (21.50)
11b86204–20656.10 (55.87)6.52 (6.81)20.13 (19.89)
11c84195–19757.52 (57.33)6.90 (7.11)19.17 (19.42)
11d 90186–18859.98 (60.11)7.55 (7.67)17.49 (17.68)