| | Compound no. | Yield, %
(%, [Lit.]) | Mp, °C (solvent)
(Mp, [Lit.]) |
(Eluent) | Empiric formula |
| | 1 | 86
(42, [17]) | 90–92 (cyclohexane)
(88–90, [17]) | 0.70
(A) | C9H13NO2S | | 2 | 81
(45, [17]) | 87–89 (hexane)
(87–89, [17]) | 0.65
(A) | C10H13NO2S | | 3 | 85
(82, [17]) | 98–100 (hexane)
(96–98, [17]) | 0.43
(B) | C11H15NO2S | | 4 | 82 | 70-71 (hexane)
(68–70, [17]) | 0.74
(B) | C12H17NO2S | | 5 | 86 | 144-145 (hexane)
(144-145, [17]) | 0.70
(A) | C11H12N2OS | | 6 | 90
(54, [14]) | 202-203 (methanol)
(200-201, [14]) | 0.65
(A) | C12H12N2OS | | 7 | 92
(60, [14]) | 214-215 (ethanol)
(212–214, [14]) | 0.43
(B) | C13H14N2OS | | 8 | 92
(62, [14]) | 157-158 (ethanol)
(156–158, [14]) | 0.74
(B) | C14H16N2OS | | 9 | 85 | 115–117 (heptane)
(115–117, [14]) | 0.75
(B) | C12H14N2OS | | 10 | 82
(80, [14]) | 182-183 (heptane)
(180–183, [14]) | 0.75
(B) | C13H14N2OS | | 11 | 88
(85, [14]) | 218–220 (ethanol)
(215-216, [14]) | 0.76
(B) | C14H16N2OS | | 12 | 92
(78, [14]) | 156–158 (ethanol)
(155–157, [14]) | 0.80
(B) | C15H18N2OS | | 13 | 88 | 159–161 (heptane)
(158–160, [15]) | 0.82
(B) | C13H16N2OS | | 14 | 85
(75, [15]) | 197-198 (heptane)
(196–198, [14]) | 0.80
(B) | C14H16N2OS | | 15 | 91
(67, [14]) | 155–157 (ethanol)
(150–152, [14]) | 0.81
(B) | C15H18N2OS | | 16 | 90
(65, [14]) | 161–163 (heptane)
(159-160, [14]) | 0.86
(B) | C16H20N2OS |
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