Research Article
Synthesis, Crystal Structure Refinement, and Electrical Conductivity of Pb(8−x)Na2Smx(VO4)6O(x/2)
Table 4
Results of elemental analysis for the samples
(wt.%).
| | V | Pb | Sm | Na | O | | exp. | theor. | exp. | theor. | exp. | theor. | exp. | theor. | exp. | theor. |
| | 0 | 13.62 | 12.77 | 69.99 | 69.26 | — | — | 1.93 | 1.92 | 14.46 | 16.05 | | 0.2 | 14.70 | 12.82 | 66.73 | 67.81 | 0.64 | 1.26 | 3.25 | 1.93 | 14.69 | 16.18 | | 0* | 12.65 | 12.77 | 68.95 | 69.26 | — | — | 1.86 | 1.92 | 16.45 | 16.05 | | 0.2* | 13.09 | 12.82 | 66.05 | 67.81 | 1.31 | 1.26 | 2.31 | 1.93 | 17.14 | 16.18 |
|
|
Elemental composition was determined using Rietveld crystal structure refinement.
|
