Research Article
Synthesis and X-Ray Structure of (1Z,2Z)-1,2-Bis(2-(phenylsulfonyl)-1-(4-tolyl)ethylidene)hydrazine
Table 1
Selected bond distances (Å), bond angles (°), and torsion angles (°) of compound 5.
| Bond distances | | | | S1–O1 | 1.419 (5) | S1–C9 | 1.766 (5) | S1–O2 | 1.424 (4) | N1–C7 | 1.290 (7) | S1–C8 | 1.792 (5) | N1–N1A | 1.419 (5) | Bond angles | | | | O1–S1–O2 | 118.6 (3) | N1i–N1–C7 | 113.8 (4) | O1–S1–C8 | 108.8 (2) | N1–C7–C6 | 116.8 (4) | O1–S1–C9 | 109.0 (3) | N1–C7–C8 | 122.8 (4) | O2–S1–C8 | 108.8 (2) | S1–C8–C7 | 112.3 (4) | O2–S1–C9 | 108.4 (2) | S1–C9–C10 | 119.6 (5) | C8–S1–C9 | 101.9 (2) | S1–C9–C14 | 119.2 (4) | Torsion angles | | | | O1–S1–C8–C7 | −43.1 (4) | C5–C6–C7–C8 | 3.8 (8) | O2–S1–C8–C7 | 87.4 (4) | C10–C9–C14–C13 | 0.2 (11) | C9–S1–C8–C7 | −158.2 (4) | S1–C9–C10–C11 | −177.3 (7) | C14–C9–S1–C8 | −97.4 (5) | C5–C6–C7–N1 | −179.3 (6) | S1–C8–C7–N1 | 91.7 (5) | | |
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Symmetry code: (i) , , .
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