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Journal of Chemistry
/
2016
/
Article
/
Tab 2
/
Research Article
Ultrasonic-Assisted Synthesis of Two
t
-Butoxycarbonylamino Cephalosporin Intermediates on SiO
2
Table 2
The effect of SiO
2
and ultrasound on the yields of the Boc-ACLE.
Number
SiO
2
Ultrasound
Reaction time
Yield%
1
✕
✕
6 h
15
2
✓
✕
6 h
35
3
✕
✓
6 h
40
4
✓
✓
30 min
96
Note:
✕
: no; ✓: yes.