Research Article

Ultrasonic-Assisted Synthesis of Two t-Butoxycarbonylamino Cephalosporin Intermediates on SiO2

Table 4

Comparison of 13C NMR data (4a).

Lee et al. reported (125 MHz, CDCl3)Synthetic 4a (75 MHz, DMSO-d6)

170.86
165.6165.01
161.4161.06
160.2159.34
154.7135.70
149.6130.25
131.0128.16
126.8126.84, 126.43
125.9125.29, 124.83
114.2113.77
81.5
68.567.28
61.259.18
58.357.96, 57.86
55.555.06
43.643.72, 40.33
28.428.93
27.426.09

Data taken from [4]; this work.