Research Article
Ultrasonic-Assisted Synthesis of Two t-Butoxycarbonylamino Cephalosporin Intermediates on SiO2
Table 4
Comparison of 13C NMR data (4a).
| Lee et al. reported (125 MHz, CDCl3) | Synthetic 4a (75 MHz, DMSO-d6) |
| — | 170.86 | 165.6 | 165.01 | 161.4 | 161.06 | 160.2 | 159.34 | 154.7 | 135.70 | 149.6 | 130.25 | 131.0 | 128.16 | 126.8 | 126.84, 126.43 | 125.9 | 125.29, 124.83 | 114.2 | 113.77 | 81.5 | — | 68.5 | 67.28 | 61.2 | 59.18 | 58.3 | 57.96, 57.86 | 55.5 | 55.06 | 43.6 | 43.72, 40.33 | 28.4 | 28.93 | 27.4 | 26.09 |
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Data taken from [4]; this work.
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