Research Article

Synthesis, Structure, and Hydrolytic Activation of Ruthenium (III)-Pyrazole Complex

Table 1

Crystal data and structure refinement for mer-[RuCl3(DMSO) (pyrazole)2] 2.

FormulaC8H14Cl3N4ORuS
Molar Mass421.71
Crystal systemMonoclinic
T (K)90
a (Ǻ)8.0596
b (Ǻ)12.6816
c (Ǻ)29.278
β (°)90.617
h, k, l limits−11 ⟶ 11; −18 ⟶ 17; −42 ⟶ 42
Z8
Θ range (°)2.5–31.0
µ (mm−1)1.72
R [F2 > 2σ(F2)]0.034
R0.038
wR(F2)0.074