Research Article
Solid State Structure of Bis[(bromo)(dicyclopentadienyl)vanadium(μ2-fluoro)][(bromo)(cyclopentadienyl)vanadium][tetrafluoroborate]
Table 1
Crystal and experimental data.
| Empirical formula | C26H27BBr3Cl2F6V3 |
| Formula weight | 927.74 | Temperature (K) | 150(1) | Wavelength () | 0.71073 | Crystal system | Monoclinic | Space group | | Unit cell dimensions | | | 7.66490(10) | | 15.2457(2) | | 13.3185(2) | β (°) | 101.2721(8) | Volume () | 1526.33(4) | | 2 | (g cm−3) | 2.019 | (MoKα) (mm−1) | 5.056 | | 900 | θ range (°) | 2.67–27.46 | Limiting indices | | | | Reflections collected/unique | 6956/3614 | Completeness (%) | 99.9 | Goodness of fit on | 1.072 | indices [] | , | indices (all data) | , | (int) | 0.0177 | | 2.374, −2.321 |
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