High Current Density Chronopotentiometric Electrosynthesis and SEM Characterization of Hexanethiol-Monolayer-Protected Silver Planar Nanotriangles (Ag@C₆SH)

Table 4

Orthogonal L₈ array design and average particle size of electrosynthesized Ag@C₆SH NCs.

Trial	Current density (A·cm^−2)	Time (Min)	Distance (mm)	Thiol conc. (mM)	Solvent ratio	Temp. (°C)	NaBH4  (w/v%)	Average size (nm)
1	0.5	15	Min.	10	50 : 50	55	0	40 (10)
2	0.5	15	Min.	20	70 : 30	75	1	43 (4)
3	0.5	30	Max.	10	50 : 50	75	1	30 (4)
4	0.5	30	Max.	20	70 : 30	55	0	35 (6)
5	0.9	15	Max.	10	70 : 30	55	1	39 (7)
6	0.9	15	Max.	20	50 : 50	75	0	44 (5)
7	0.9	30	Min.	10	70 : 30	75	0	41 (4)
8	0.9	30	Min.	20	50 : 50	55	1	37 (5)