Review of the Design and Operation Criteria of a DC Submerged Arc Discharge Carbon Nanostructure Synthesis Installation
Table 4
Control of sensitive parameters.
Temporal evolution
Parameters
Importance of control
Slow changes
pH
It provides indirect information about the processes that occur and the stability of the colloid systems that arise
Liquid temperature
A sufficiently low temperature prevents evaporation, provides a high liquid viscosity that increases vibration damping, and minimizes expansion of system components
Liquid level
A constant water level in the reactor guarantees a constant pressure on the bubbles and a constant heat capacity. This contributes to the homogeneity of the characteristics of the CNSs
Fast changes
Sound emission
Contactless diagnosis. Vibrations of system components, bubble size, and chemical reactions present
Light emission
Provides information about the environment of the discharge and in certain circumstances about the species present in it