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Organic Chemistry International
Table of Contents
Organic Chemistry International
/
2014
/
Article
/
Sch 2
/
Research Article
Stereoselective Synthesis of (+)-
-Conhydrine from
R
-(+)-Glyceraldehyde
Scheme 2
Reagent and conditions: (a) CH
2
=CHCH
2
NH
2
, Et
2
O, anhyd.MgSO
4
, 0°C to rt, 3 h, 82%; (b) CH
2
=CHCH
2
Br, Zn, THF, aq.NH
4
Cl, 0°C to rt, 10 h, 80%.