Research Article

A Novel One-Pot and One-Step Microwave-Assisted Cyclization-Methylation Reaction of Amino Alcohols and Acetylated Derivatives with Dimethyl Carbonate and TBAC

Table 1

Synthesis of 4-substituted-3-methyl-1,3-oxazolidin-2-ones.

ā€‰634935.table.001a

EntryStarting materialProductYield (%)a,b

1634935.table.001b634935.table.001c79

2634935.table.001d634935.table.001e79

3634935.table.001f634935.table.001g81

4634935.table.001h634935.table.001i82

5634935.table.001j634935.table.001k80

6634935.table.001l634935.table.001m93

7634935.table.001n634935.table.001o95

Isolated yields based on the starting amino alcohol. bProducts characterized by 1H and 13C NMR.