Research Article
Synthesis and Characterization of Bis(4-methylbenzylammonium) Tetrachloridocadmate(II)
Table 1
Cristallographic data and refinement details of the title compound.
| | CdCl4ยท(C8H12N)2 | F(000) = 1000.00 | | = 498.57 | = 1.706 Mg mโ3 | | Orthorhombic, Pnma | Mo Kฮฑ radiation, ฮป = 0.71073โร
| | a = 10.721 (2) ร
| Cell parameters from 670 reflections | | b = 33.986 (6) ร
| ฮธ = 2.4โ31.3ยฐ | | c = 5.326(1) ร
| ฮผ = 1.68โcmโ1 | | ฮฒ = 97.222 (1)ยฐ | T = 289โK | | V = 1940.8(7) ร
3 | Crystal size: 0.009 ร 0.08 ร 0.06โmm | | Z = 4 | 2856 independent reflections | | ฯ and ฯ scans | 2278 reflections with | | = 0.608, = 0.746 | = 0.023 | | Color: colourless | = 30.1ยฐ, = 3.6ยฐ | | Goodness-of-fit on โ:โ1.1 | | | 6959 measured reflections | | | Refinement on | | | = 0.041 | where | | wR(F2) = 0.093 | (ฮ/ฯ)max = 0.001 | | 11674 reflections | ฮฯ max = 1.23โeโร
โ3 | | 111 parameters | ฮฯ min = โ1.78โeโร
โ3 |
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