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Bioinorganic Chemistry and Applications

Bioinorganic Chemistry and Applications / 2010 / Article / Tab 2

Research Article

Hydrogen-Bonded Networks Based on Cobalt(II), Nickel(II), and Zinc(II) Complexes of N,N'-Diethylurea

Table 2

Selected bond lengths ( ) and angles (°) for 1.
Co–O( )2.094(2)N(11)–C(13)1.327(5)
Co–O(11)2.088(2)C(13)–N(12)1.323(5)
Co–O(21)2.112(2)N(12)–C(14)1.456(7)
O( )–C(3)1.262(4)C(14)–C(15)1.417(8)
O(11)–C(13)1.267(4)C(21)–C(22)1.451(8)
O(21)–C(23)1.256(4)C(22)–N(21)1.456(5)
C( )–C(2)1.486(6)N(21)–C(23)1.325(5)
C(2)–N( )1.450(5)C(23)–N(22)1.335(5)
N( )–C(3)1.331(5)N(22)–C(24)1.450(6)
C(3)–N(2)1.325(5)C(24)–C(25)1.390(9)
N(2)–C(4)1.462(7)B–F( )1.279(6)
C(4)–C(5)1.372(9)B–F(2)1.311(9)
C(11)–C(12)1.289(9)B–F(3)1.331(8)
C(12)–N(11)1.459(6)B–F(4)1.265(10)
O(11)#1–Co–O(11)180.00(19)C(3)–N(2)–C(4)124.0(4)
O(11)#1–Co–O( )92.93(10)C(5)–C(4)–N(2)111.7(6)
O(11)–Co–O( )87.07(10)C(11)–C(12)–N(11)119.0(7)
O(11)#1–Co–O( )#187.07(10)C(13)–N(11)–C(12)126.9(4)
O(11)–Co–O( )#192.93(10)O(11)–C(13)–N(12)119.6(4)
O( )–Co–O( )#1180.00(8)O(11)–C(13)–N(11)120.4(3)
O(11)#1–Co–O(21)#186.69(10)N(12)–C(13)–N(11)120.0(4)
O(11)–Co–O(21)#193.31(10)C(13)–N(12)–C(14)125.1(4)
O( )–Co–O(21)#187.20(10)C(15)–C(14)–N(12)112.8(6)
O( )#1–Co–O(21)#192.80(10)C(21)–C(22)–N(21)113.9(5)
O(11)#1–Co–O(21)93.31(10)C(23)–N(21)–C(22)127.9(4)
O(11)–Co–O(21)86.69(10)O(21)–C(23)–N(21)121.0(3)
O( )–Co–O(21)92.80(10)O(21)–C(23)–N(22)120.1(3)
O( )#1–Co–O(21)87.20(10)N(21)–C(23)–N(22)119.0(3)
O(21)#1–Co–O(21)180.00(12)C(23)–N(22)–C(24)124.3(4)
C(3)–O( )–Co132.5(2)C(25)–C(24)–N(22)114.1(6)
C(13)–O(11)–Co127.6(2)F(4)–B–F( )111.2(9)
C(23)–O(21)–Co129.7(2)F(4)–B–F(2)103.0(7)
N( )–C(2)–C( )111.0(4)F( )–B–F(2)115.0(6)
C(3)-N( )-C(2)125.8(3)F(4)-B-F(3)105.1(8)
O( )-C(3)-N(2)119.9(4)F( )-B-F(3)115.1(5)
O( )-C(3)-N( )121.2(3)F(2)-B-F(3)106.3(7)
N(2)-C(3)-N( )118.9(4)
Symmetry transformation used to generate equivalent atoms: #1 , , .

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