Research Article

Metal-Based Biologically Active Compounds: Synthesis, Spectral, and Antimicrobial Studies of Cobalt, Nickel, Copper, and Zinc Complexes of Triazole-Derived Schiff Bases

Table 4

Thermoanalytical results (TG) of the metal complexes.

CompoundStepsTemp. (°C)TG mass%Assignments
Calcd.Found

Cu(L2)21st
2nd
3rd
80–305
305–505
505–695
47.90
21.26
21.26
11.98
45.29
20.27
20.05
15.16
−C14H8Cl4 (organic moiety)
−C4H5N4S (triazole ring)
−C4H5N4S (triazole ring)
−CuO (residue)
Zn(L1)2·2H2O1st
2nd
3rd
80–230
230–560
560–700
5.37
51.30
33.73
11.90
4.98
51.50
31.12
12.40
−H4O2 (two water molecule)
−C14H8Cl4N2 (organic moiety)
−C6H6N6S2 (triazole ring)
−ZnO (residue)