Research Article
Synthesis and Crystal Structure of the Bioinorganic Complex [Sb(Hedta)]·2H2O
Table 4
Experimental data and calculated results for powder X-ray diffraction pattern of the complex [Sb(Hedta)]·2H
2O (orthorhombic system:
Å,
Å, and
Å).
| | No. | (°) | | | | (Å) | (Å) | |
| | 1 | 9.56 | 2 | 0 | 0 | 9.242 | 9.240 | 100.0 | | 2 | 12.52 | 2 | 1 | 0 | 7.064 | 7.063 | 1.5 | | 3 | 12.96 | 1 | 0 | 1 | 6.827 | 6.824 | 1.2 | | 4 | 14.51 | 0 | 1 | 1 | 6.100 | 6.100 | 9.5 | | 5 | 15.30 | 1 | 1 | 1 | 5.788 | 5.792 | 42.6 | | 6 | 16.17 | 0 | 2 | 0 | 5.477 | 5.478 | 1.6 | | 7 | 16.85 | 1 | 2 | 0 | 5.256 | 5.253 | 17.2 | | 8 | 17.41 | 2 | 1 | 1 | 5.090 | 5.091 | 5.2 | | 9 | 18.11 | 2 | 2 | 0 | 4.713 | 4.712 | 2.1 | | 10 | 19.19 | 4 | 0 | 0 | 4.621 | 4.620 | 8.5 | | 11 | 20.48 | 3 | 1 | 1 | 4.332 | 4.334 | 5.5 | | 12 | 20.85 | 4 | 1 | 0 | 4.257 | 4.257 | 9.7 | | 13 | 21.69 | 3 | 2 | 0 | 4.094 | 4.094 | 3.0 | | 14 | 22.40 | 2 | 2 | 1 | 3.966 | 3.966 | 4.5 | | 15 | 24.15 | 4 | 1 | 1 | 3.682 | 3.683 | 2.7 | | 16 | 24.86 | 1 | 3 | 0 | 3.579 | 3.583 | 0.9 | | 17 | 26.10 | 2 | 0 | 2 | 3.411 | 3.412 | 2.8 | | 18 | 27.37 | 2 | 1 | 2 | 3.256 | 3.258 | 1.8 | | 19 | 28.21 | 3 | 0 | 2 | 3.160 | 3.154 | 5.9 | | 20 | 28.95 | 6 | 0 | 0 | 3.081 | 3.080 | 9.4 | | 21 | 29.69 | 1 | 2 | 2 | 3.007 | 3.009 | 11.8 | | 22 | 31.12 | 4 | 0 | 2 | 2.871 | 2.874 | 10.6 | | 23 | 31.61 | 5 | 2 | 1 | 2.828 | 2.828 | 1.3 | | 24 | 32.73 | 3 | 2 | 2 | 2.733 | 2.733 | 5.0 | | 25 | 33.00 | 1 | 4 | 0 | 2.712 | 2.710 | 3.6 | | 26 | 33.54 | 4 | 3 | 1 | 2.670 | 2.669 | 1.1 | | 27 | 34.10 | 2 | 4 | 0 | 2.627 | 2.626 | 3.4 | | 28 | 35.24 | 1 | 4 | 1 | 2.544 | 2.542 | 1.1 | | 29 | 35.84 | 3 | 4 | 0 | 2.503 | 2.503 | 3.5 | | 30 | 37.07 | 1 | 0 | 3 | 2.423 | 2.426 | 10.2 | | 31 | 37.80 | 7 | 2 | 0 | 2.378 | 2.378 | 3.0 | | 32 | 38.11 | 2 | 0 | 3 | 2.360 | 2.366 | 6.7 | | 33 | 38.95 | 2 | 1 | 3 | 2.311 | 2.313 | 3.4 | | 34 | 39.81 | 4 | 3 | 2 | 2.262 | 2.259 | 0.8 | | 35 | 40.18 | 4 | 4 | 1 | 2.242 | 2.244 | 2.5 | | 36 | 40.50 | 1 | 2 | 3 | 2.225 | 2.219 | 1.2 | | 37 | 40.95 | 0 | 4 | 2 | 2.202 | 2.196 | 0.9 | | 38 | 41.39 | 2 | 2 | 3 | 2.178 | 2.172 | 1.7 | | 39 | 41.77 | 4 | 0 | 3 | 2.161 | 2.163 | 1.2 | | 40 | 42.28 | 7 | 0 | 2 | 2.137 | 2.143 | 1.1 | | 41 | 43.31 | 1 | 5 | 1 | 2.087 | 2.086 | 1.9 | | 42 | 45.19 | 4 | 2 | 3 | 2.006 | 2.012 | 1.3 | | 43 | 45.69 | 2 | 3 | 3 | 1.984 | 1.986 | 4.1 | | 44 | 46.62 | 8 | 3 | 0 | 1.947 | 1.952 | 1.3 | | 45 | 47.18 | 3 | 3 | 3 | 1.926 | 1.931 | 1.2 | | 46 | 48.17 | 5 | 4 | 2 | 1.888 | 1.888 | 1.8 | | 47 | 48.93 | 4 | 3 | 3 | 1.860 | 1.861 | 1.8 | | 48 | 49.89 | 0 | 4 | 3 | 1.826 | 1.825 | 1.9 | | 49 | 50.90 | 2 | 4 | 3 | 1.792 | 1.791 | 1.0 | | 50 | 53.92 | 4 | 4 | 3 | 1.698 | 1.697 | 1.3 | | 51 | 58.45 | 3 | 6 | 2 | 1.578 | 1.580 | 0.8 | | 52 | 58.77 | 0 | 7 | 0 | 1.569 | 1.565 | 0.8 | | 53 | 59.94 | 2 | 7 | 0 | 1.542 | 1.543 | 1.2 | | 54 | 60.66 | 0 | 4 | 4 | 1.525 | 1.525 | 1.1 | | 55 | 61.79 | 5 | 3 | 4 | 1.500 | 1.499 | 0.9 | | 56 | 64.46 | 2 | 1 | 5 | 1.442 | 1.438 | 0.9 | | 57 | 67.57 | 2 | 5 | 4 | 1.388 | 1.391 | 0.9 |
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