Synthesis and Crystal Structure of the Bioinorganic Complex [Sb(Hedta)]·2H₂O

Table 5

Thermal decomposition data of the title complex.

Reaction	DSC (°C)	Mass loss (%)
		𝑊exp	𝑊theor
[Sb(Hedta)]·2H2O
↓ −2H2O	81 (endo.)	8.14	8.06
[Sb(Hedta)]
↓ structural rearrangement	294 (endo.)
[Sb(Hedta)]
↓ −C8.5H13N2O3.5	330 (exo.)	44.55	44.57
1/2Sb2(CO3)3
↓ −C3O5	492 (exo.)	12.85	12.98
1/2Sb2O4
↓ −Sb0.5O1.25	534 (endo.)	19.11	18.09
1/4Sb2O3		15.35^a	16.30^b

aThe experimental percentage mass of the residue in the sample; ^bthe calculated percentage mass of the residue in the sample.