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Bioinorganic Chemistry and Applications
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Bioinorganic Chemistry and Applications
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2014
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Article
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Tab 4
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Research Article
Metal (II) Complexes Derived from Naphthofuran-2-carbohydrazide and Diacetylmonoxime Schiff Base: Synthesis, Spectroscopic, Electrochemical, and Biological Investigation
Table 4
Thermogravimetric data of Ni(II), Cu(II), and Cd(II) complexes.
Empirical formulae of the complexes
Decomposition temperature (°C)
Weight loss (%)
Metal oxide (%)
Inference
Found
Calc.
Found
Calc.
Ni(C
17
H
15
O
3
N
3
)Cl
2
312–314
15.59
15.95
13.12
13.61
Loss of chloride molecules
345–347
70.09
70.44
Loss of ligand
Cu(C
17
H
15
O
3
N
3
)
2
Cl
2
209–211
8.95
9.29
8.14
8.43
Loss of chloride molecules
259–261
22.23
22.61
Loss of oxime moiety
438–440
59.10
59.51
Loss of furan moiety
Cd(C
17
H
15
O
3
N
3
)Cl
2
278–280
13.85
14.21
22.85
23.02
Loss of chloride molecules
389–391
62.32
62.76
Loss of ligand