Research Article

Active Microbial Communities Inhabit Sulphate-Methane Interphase in Deep Bedrock Fracture Fluids in Olkiluoto, Finland

Table 2

Geochemical analysis methods and the detection limit of each assay used in this study. The data were obtained from Posiva Oy.

ParameterUnitMethodDetection limit

pHpH meter, ISO-10532
EC (mS m−1)Conductivity analyzer, SFS-EN-278885
NPOC(mg L−1)SFS-EN 1484TC: 0.6
IC: 0.3 l
TOC: 0.3
TDS(mg L−1)
Alk(meq L−1)Titration with HCl0.05
(mg L−1)IC, conductivity detector0.1
S2−(mg L−1)Spectrophotometry0.1
(mg L−1)FIA method, SFS-EN ISO11905-10.05
(mg L−1)Spectrophotometry, SFS 3032
Fe2+(mg L−1)Spectrophotometry0.01
Na2+(mg L−1)2007: FAAS, SFS3017, 3044
2008: ICP-OES
5
0.5
K+(mg L−1)2007: FAAS, SFS3017, 3044
2008: ICP-OES
0.31
0.5
Ca2+(mg L−1)2007: FAAS, SFS3017, 3044
2008: ICP-OES
0.02
0.1
Mg2+(mg L−1)2007: FAAS, SFS3018
2008: ICP-OES
0.15
0.02
Cl(mg L−1)Titration5
CH4(mL L−1 gas)Gas chromatography1 L L−1 gas