Micro-Raman Vibrational Identification of 10-MDP Bond to Zirconia and Shear Bond Strength Analysis

Table 1

Spreading of materials’ composition and manufacturers.

Materials	Composition	Manufacturer
Zirconcad	99.0% ZrO2 + Y2O3; 0.5% Y2O3	Angelus, Londrina, Brazil
RelyX ARC	Paste A: Bis-GMA, TEGDMA, silane treated silica, functionalized dimethacrylate polymer, 2-benzotriazolyl-4-methylphenol, 4-(dimethylamino)-benzeneethanol.; Paste B: silane treated ceramic, TEGDMA, Bis-GMA, silane treated silica, functionalized dimethacrylate polymer, 2-benzotriazolyl-4-methylphenol, benzoyl peroxide (72/wt).	3M ESPE, St. Paul, USA
RelyX U200	Base: Methacrylate monomers containing phosphoric acid groups, methacrylate monomers, initiators, stabilizers, rheological additives.; Catalyst: Methacrylate monomers, alkaline fillers, silanated fillers, initiator components, stabilizers, pigments, rheological additives. Zirconia/silica fillers	3M ESPE, St. Paul, USA
Clearfil Ceramic Primer	10-Methacryloyloxydecyl dihydrogen phosphate, 3-(trimethoxysilyl)propyl methacrylate, ethanol	Kuraray Medical Inc., Tokyo, Japan