Chromatography Research International / 2013 / Article / Tab 2

Research Article

A Comparative Validation Study of Fluconazole by HPLC and UPLC with Forced Degradation Study

Table 2

Robustness study data obtained from HPLC.

Robustness conditionsRT (min)ASSAY (%)System suitability data
Type RateTheoretical plateAsymmetry

Flow rate0.9 mL/min.3.59100.0934980.97
1.1 mL/min.2.9599.8436071.03
Temperature28°C3.2498.9739301.07
32°C3.2299.6838901.50
Mobile phase72 : 283.16101.0740271.67
68 : 323.3299.4241451.09

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