Chromatography Research International / 2013 / Article / Tab 3

Research Article

A Comparative Validation Study of Fluconazole by HPLC and UPLC with Forced Degradation Study

Table 3

Robustness study data obtained from UPLC analysis.

Robustness conditionsRT (min)ASSAY (%)System suitability data
Type RateTheoretical plateAsymmetry

Flow rate0.28 mL/min.1.2599.8527921.06
0.32 mL/min.1.06101.9924600.71
Temperature281.0598.9523610.97
321.2499.5531941.67
Mobile phase53 : 471.2698.6029841.05
57 : 431.1199.5127891.10

Article of the Year Award: Outstanding research contributions of 2020, as selected by our Chief Editors. Read the winning articles.