Table of Contents
Chromatography Research International
Volume 2016, Article ID 1596021, 7 pages
http://dx.doi.org/10.1155/2016/1596021
Research Article

Validated Stability Indicating Chromatographic Method for the Simultaneous Estimation of Camylofin with NSAID Drugs and a New Approach of Method Transfer from Classical HPLC to a Modern UPLC Instrument

1Center of Excellence in Drug Discovery, NFDD Complex, Department of Chemistry, Saurashtra University, Rajkot, Gujarat 360005, India
2Matushri Virbaima Mahila Science & Home Science College, Rajkot, India

Received 27 April 2016; Revised 13 September 2016; Accepted 19 September 2016

Academic Editor: Susana Casal

Copyright © 2016 Sheetal Makwana et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Linked References

  1. Sweetman and C. Sean, Martindale, The Complete Drug Reference, 36th edition, 2009.
  2. F. A. Elbarbry, M. M. Mabrouk, and M. A. El‐Dway, “Determination of the analgesic components of Spasmomigraine tablet by liquid chromatography with ultraviolet detection,” Journal of AOAC International, vol. 90, pp. 94–101, 2007. View at Google Scholar
  3. M. J. O'Neil, A. Smith, P. E. Heckelman, J. R. Obenchain Jr., A. R. Gallipeau, and M. Ann D'Arecca, The Merck Index: An Encyclopedia of Chemicals, Drugs, and Biological, Merck, Rahway, NJ, USA, 13th edition, 2001.
  4. N. M. Davies and K. E. Anderson, “Clinical pharmacokinetics of diclofenac. Therapeutic insights and pitfalls,” Clinical Pharmacokinetics, vol. 33, no. 3, pp. 184–213, 1997. View at Publisher · View at Google Scholar
  5. C. Dollery, Therapeutic Drugs, Churchill Livingstone, Edinburgh, Scotland, 2nd edition, 1999.
  6. S. C. Sweetman, The Martindale: The Complete Drug Reference, Pharmaceutical Press, London, UK, 35th edition, 2006.
  7. L. B. Laurence and J. S. Lozo, “Analgesics, antipyretic and anti-inflammatory agents,” in Goodman & Gilman's the Pharmacological Basis of Therapeutics, pp. 671–675, Medical Publishing, Division, New York, NY, USA, 11th edition, 2006. View at Google Scholar
  8. S. Budavari, Ed., The Merck Index: An Encyclopedia of Chemicals, Drugs, and Biologicals, Merck and Co., Inc, White House Station, NJ, USA, 2001.
  9. United States Pharmacopeia, National Formulary 25, United States Pharmacopeia, Rockville, Md, USA, 2007.
  10. A. Jawad, Hepatology and Transplant Hepatology: A Case Based Approach, Springer Science & Business Media, New York, NY, USA, 2010.
  11. Acetaminophen, The American Society of Health-System Pharmacists, http://www.drugs.com/monograph/acetaminophen.html
  12. S. Makwana, M. Patel, B. Singh, J. Upadhyay, and A. Shah, “Development and validation of a stability indicating RP-UPLC method for the determination of Paracetamol and Ibuprofen in tablet,” Journal of Chemical and Pharmaceutical Research, vol. 7, no. 4, pp. 1308–1315, 2015. View at Google Scholar
  13. R. R. Singh, M. V. Rathnam, S. J. Singh, and R. V. K. Vegesna, “A stability indicating gc-fid method for camylofin dihydrochloride and diclofenac potassium in pharmaceutical preparation,” International Journal of Pharmacy and Pharmaceutical Sciences, vol. 4, no. 1, pp. 317–324, 2012. View at Google Scholar · View at Scopus
  14. N. N. Kadam, P. C. Patil, and R. R. Singh, “A stability-indicating RP-HPLC determination of camylofin dihydrochloride in drug substance,” International Journal of Pharmacy and Pharmaceutical Sciences, vol. 3, no. 3, pp. 153–158, 2011. View at Google Scholar · View at Scopus
  15. N. S. Patel, V. P. Gandh, R. S. Mehta, and K. K. Bhatt, “Application of HPLC and HPTLC-densitometry for the simultaneous determination of camylofin and diclofenac in pharmaceutical dosage form,” Der Pharmacia Lettre, vol. 2, no. 5, pp. 193–207, 2010. View at Google Scholar
  16. R. R. Singh, M. V. Rathnam, and R. Vegesna, “Simultaneous RP HPLC determination of Camylofin dihydrochloride and paracetamol in pharmaceutical preparations,” TSI Journal, vol. 7, no. 11, 2008. View at Google Scholar
  17. B. Anupama and V. Ramakrishna, “New visible spectrophotometric methods for determination of camylofin,” International Journal of Research in Pharmacy and Chemistry, vol. 2, no. 4, pp. 1020–1022, 2012. View at Google Scholar
  18. ICH Guideline, Q2 (R1) Step 4, Validation of Analytical Procedures: Text and Methodology, 2005.
  19. USP, United States Pharmacopoeia, United States Pharmacopeial Convention, Rockville, Md, USA, 30th edition, 2007.
  20. AOAC Peer-Verified Methods Program, Manual on Policies and Procedures, AOAC International, Arlington, Va, USA, 1998.
  21. ICH Guidelines, “Q1A (R2): stability testing of new drug substances and products (revision 2),” in Proceedings of the International Conference on Harmonization, November 2003, http://www.fda.gov/downloads/drugs/guidancecomplianceregulatoryinformation/guidances/ucm073369.pdf.