QuEChERS Method Followed by Solid Phase Extraction Method for Gas Chromatographic-Mass Spectrometric Determination of Polycyclic Aromatic Hydrocarbons in Fish

Table 3

Representing recovery percentage, relative standard deviation (RSD%), and RSD_pooled% results of replicates on each spiking level.

Compounds	Recovery ± RSD%			RSDpooled%
	2.0 µg/Kg	10.0 µg/Kg	50.0 µg/Kg
(1) Naphthalene				5
(2) Acenaphthene				5
(3) Acenaphthylene				4
(4) Fluorene				5
(5) Phenanthrene				5
(6) Anthracene				5
(7) Fluoranthene				5
(8) Pyrene				5
(9) Benzo(a)anthracene				2
(10) Chrysene				4
(11) Benzo(b)fluoranthene				3
(12) Benzo(k)fluoranthene				4
(13) Benzo(a)pyrene				4
(14) Indeno(1,2,3-cd)pyrene				4
(15) Dibenzo(a,h)anthracene				4
(16) Benzo(g,h,i)perylene				4