International Journal of Analytical Chemistry / 2015 / Article / Tab 3

Research Article

QuEChERS Method Followed by Solid Phase Extraction Method for Gas Chromatographic-Mass Spectrometric Determination of Polycyclic Aromatic Hydrocarbons in Fish

Table 3

Representing recovery percentage, relative standard deviation (RSD%), and RSDpooled% results of replicates on each spiking level.

CompoundsRecovery ± RSD%RSDpooled%
2.0 µg/Kg10.0 µg/Kg50.0 µg/Kg

(1) Naphthalene5
(2) Acenaphthene5
(3) Acenaphthylene4
(4) Fluorene5
(5) Phenanthrene5
(6) Anthracene5
(7) Fluoranthene5
(8) Pyrene5
(9) Benzo(a)anthracene2
(10) Chrysene4
(11) Benzo(b)fluoranthene3
(12) Benzo(k)fluoranthene4
(13) Benzo(a)pyrene4
(14) Indeno(1,2,3-cd)pyrene4
(15) Dibenzo(a,h)anthracene4
(16) Benzo(g,h,i)perylene4

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