International Journal of Analytical Chemistry / 2015 / Article / Tab 4

Research Article

A High Throughput Method for Measuring Polycyclic Aromatic Hydrocarbons in Seafood Using QuEChERS Extraction and SBSE

Table 4

Analysis on SRM mussel tissue.

AnalyteAcceptable range (ng/g)Certificate of analysis (ng/g)QuEChERS-SBSE (ng/g)%RSD

Naphthalene1.6–3.32.41.018.5
Fluorene0.3–0.70.490.35114.7
Phenanthrene1.7–3.52.61.911.1
Anthracene0.3–0.80.532.4215.2
Fluoranthene11.5–23.11719.27.0
Pyrene12.2–24.21819.07.2
Benzanthracene2.9–6.94.73.77.2
Chrysene + Triphenylene7.4–13.810.68.86.8
Benzopyrene2.0–3.62.81.710.4

Total59.1258.05

= 3 (only detected using 60 m column).
2Possible coelution.

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