International Journal of Inorganic Chemistry

Volume 2010, Article ID 326568, 6 pages

http://dx.doi.org/10.1155/2010/326568

Research Article

## Syntheses and Crystal Structures of and

Department of Applied Molecular Chemistry, College of Industrial Technology, Nihon University, Izumi, Narashino, Chiba 275-8575, Japan

Received 31 August 2009; Accepted 10 November 2009

Academic Editor: J. D. Woollins

Copyright © 2010 Takayoshi Fujii et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

#### Linked References

- O. Glemser and R. Mews, “Chemistry of thiazyl fluoride (NSF) and thiazyl trifluoride (${\text{NSF}}_{3}$): a quarter century of sulfur-nitrogen-fluorine chemistry,”
*Angewandte Chemie International Edition*, vol. 19, no. 11, pp. 883–899, 1980. View at Google Scholar - U. Behrens, E. Lork, J. Petersen, A. Waterfeld, and R. Mews, “Thiazyltrifluoride ${\text{NSF}}_{3}$ and thiazyldifluoridedimethylamide ${\text{NSF}}_{2}{\text{NMe}}_{2}$: ligands in organometallic chemistry,”
*Zeitschrift für Anorganische und Allgemeine Chemie*, vol. 623, no. 10, pp. 1518–1524, 1997. View at Google Scholar · View at Scopus - R. Mews, E. Lork, P. G. Watson, and B. Görtler, “Coordination chemistry in and of sulfur dioxide,”
*Coordination Chemistry Reviews*, vol. 197, no. 1, pp. 277–320, 2000. View at Google Scholar · View at Scopus - R. Mews, T. Borrmann, R. Hoppenheit et al., “Fluorothiazynes, 50 years old and still exciting: electrophilic attack at the thiazyl nitrogen of ${\text{NSF}}_{2}\text{NS}(\text{O}){\text{F}}_{2}$,”
*Journal of Fluorine Chemistry*, vol. 125, no. 11, pp. 1649–1655, 2004. View at Publisher · View at Google Scholar · View at Scopus - T. Yoshimura, K. Hamada, M. Imado et al., “First preparation and X-ray crystallographic structure determination of $S$,$S$,$S$-triphenylthiazyne,”
*The Journal of Organic Chemistry*, vol. 62, no. 12, pp. 3802–3803, 1997. View at Google Scholar · View at Scopus - T. Yoshimura, M. Ohkubo, T. Fujii et al., “Synthesis, structure, and thermolysis mechanism of $S$-alkoxythiazynes,”
*Bulletin of the Chemical Society of Japan*, vol. 71, no. 7, pp. 1629–1637, 1998. View at Google Scholar · View at Scopus - T. Yoshimura, T. Fujii, S. Murotani et al., “The structures of ${[{\text{Ph}}_{2}{\text{XS-N-SPh}}_{2}\text{NH}]}^{+}$ cations (X=NH, O),”
*Journal of Organometallic Chemistry*, vol. 611, no. 1-2, pp. 272–279, 2000. View at Google Scholar · View at Scopus - T. Fujii, T. Fujimori, S. Miyoshi, S. Murotani, M. Ohkubo, and T. Yoshimura, “The structures of diphenyl(diphenylsulfimido) (nitrido)sulfur(VI) and diphenyl(diphenylsulfodiimido)(nitrido)sulfur(VI), ${\text{Ph}}_{2}(\text{X})\text{S=N-}({\text{Ph}}_{2})\text{S}\equiv \text{N}$ (X = lone pair, NH),”
*Heteroatom Chemistry*, vol. 12, no. 4, pp. 263–268, 2001. View at Google Scholar · View at Scopus - T. Fujii, A. Itoh, K. Hamata, and T. Yoshimura, “First preparation and crystal structure of heterocyclic ${\lambda}^{6}$-sulfanenitrile, 2,${2}^{\prime}$-biphenylylene(phenyl)-${\lambda}^{6}$-sulfanenitrile,”
*Tetrahedron Letters*, vol. 42, no. 30, pp. 5041–5043, 2001. View at Publisher · View at Google Scholar · View at Scopus - T. Fujii, T. Suzuki, T. Sato, E. Horn, and T. Yoshimura, “Synthesis, structure, and reactivity of iminosulfonium ylides bearing an $\alpha $-carbonyl group,”
*Tetrahedron Letters*, vol. 42, no. 35, pp. 6151–6154, 2001. View at Publisher · View at Google Scholar · View at Scopus - T. Fujii, T. Ikeda, T. Mikami, T. Suzuki, and T. Yoshimura, “Synthesis and structure of $(\text{MeN}){\text{Ph}}_{2}{\text{S=C=SPh}}_{2}(\text{NMe})$,”
*Angewandte Chemie International Edition*, vol. 41, no. 14, pp. 2576–2578, 2002. View at Publisher · View at Google Scholar · View at Scopus - T. Fujii, S. Asai, T. Okada, W. Hao, H. Morita, and T. Yoshimura, “A new method for the preparation of fluoro-${\lambda}^{6}$-sulfanenitriles: reaction of sulfimides with ${\text{selectfluor}}^{\text{TM}}$,”
*Tetrahedron Letters*, vol. 44, no. 33, pp. 6203–6205, 2003. View at Publisher · View at Google Scholar · View at Scopus - T. Fujii, M. Kanno, M. Hirata, T. Fujimori, and T. Yoshimura, “Synthesis and properties of ${\text{Ph}}_{2}\text{S}{(\text{=N-}({\text{Ph}}_{2})\text{S}\equiv \text{N})}_{2}$,”
*Inorganic Chemistry*, vol. 44, no. 24, pp. 8653–8655, 2005. View at Publisher · View at Google Scholar · View at PubMed · View at Scopus - T. Fujii, T. Takano, S. Asai, H. Morita, M. Hirata, and T. Yoshimura, “10-Oxo-10$H$-5${\lambda}^{4}$,10${\lambda}^{4}$-thianthren-5-ylideneamine as a probe for stereochemistry in the formation and amination of fluoro-${\lambda}^{6}$-sulfanenitriles,”
*Tetrahedron*, vol. 62, no. 41, pp. 9622–9627, 2006. View at Publisher · View at Google Scholar · View at Scopus - T. Fujii, M. Kanno, M. Hirata, T. Nakahodo, T. Wakahara, and T. Akasaka, “Synthesis and characterization of Co(II), Ni(II), and Cu(II) complexes containing an eight-membered disulfanenitrile chelating ring,”
*Inorganica Chimica Acta*, vol. 361, no. 8, pp. 2540–2546, 2008. View at Publisher · View at Google Scholar · View at Scopus - T. Fujii, S. Iwata, M. Hirata et al., “Syntheses and crystal structures of $[{\text{ClPh}}_{2}\text{Sn}\{\text{E}{({\text{Ph}}_{2}\text{SN})}_{2}\}](\text{E=CH,N})$,”
*Phosphorus, Sulfur and Silicon and the Related Elements*. In press. - G. M. Sheldrick, “A short history of SHELX,”
*Acta Crystallographica Section A*, vol. 64, no. 1, pp. 112–122, 2008. View at Publisher · View at Google Scholar · View at PubMed · View at Scopus - T. Yoshimura, T. Fujii, and H. Dai, “Synthesis and crystal structures of ${[{\text{CuCl}}_{2}(\mu {\text{-NSPh}}_{3})]}_{2}$ and $[{\text{CuCl}}_{2}{({\text{Ph}}_{3}\text{SN})}_{2}]$: novel copper complexes bearing organic ${\lambda}^{6}$-sulfanenitrile as ligand,”
*Chemistry Letters*, vol. 31, no. 10, pp. 1000–1001, 2002. View at Google Scholar · View at Scopus