Research Article
Synthesis and Characterization of Bis(4-methylbenzylammonium) Tetrachloridocadmate(II)
Table 3
Selected bond angles (°) in [4-CH3C6H4CH2NH3]2[CdCl4].
| Cl2–Cd1–Cl2i | 174.05 (7) | C2–C7–C6 | 121.8 (4) | Cl2–Cd1–Cl3 | 92.92 (3) | N1–C1–H1A | 109.0 | Cl2i –Cd1–Cl3 | 92.92 (3) | C2–C1–H1A | 109.0 | Cl2–Cd1–Cl1 | 90.87 (3) | N1–C1–H1B | 109.0 | Cl2i –Cd1–Cl1 | 90.87 (3) | C2–C1–H1B | 109.0 | Cl3–Cd1–Cl1 | 84.62 (5) | C5–C8–H8C | 109.5 | Cl2–Cd1–Cl1ii | 89.36 (3) | C1–N1–H1C | 109.5 | Cl2i –Cd1–Cl1ii | 89.35 (3) | C1–N1–H1D | 109.5 | Cl3–Cd1–Cl1ii | 90.92 (5) | C4–C3–H3 | 119.6 | Cl1–Cd1–Cl1ii | 175.54 (7) | C2–C3–H3 | 119.6 | Cl2–Cd1–Cl3iii | 87.12 (3) | C3–C4–H4 | 119.5 | Cl2i –Cd1–Cl3iii | 87.12 (3) | C5–C4–H4 | 119.5 | Cl3–Cd1–Cl3iii | 177.204 (13) | C1–N1–H1E | 109.5 | Cl1–Cd1–Cl3iii | 92.58 (5) | C7–C6–H6 | 119.8 | Cl1ii –Cd1–Cl3iii | 91.88 (5) | C5–C6–H6 | 119.8 | Cd1–Cl1–Cd1iv | 175.54 (7) | C2–C7–H7 | 119.1 | Cd1–Cl3–Cd1v | 176.50 (7) | C6–C7–H7 | 119.1 | N1–C1–C2 | 113.1 (4) | C5–C8–H8A | 109.5 | C7–C2–C3 | 118.1 (4) | C5–C8–H8B | 109.5 | C7–C2–C1 | 121.0 (4) | H8A–C8–H8C | 109.5 | C3–C2–C1 | 120.9 (4) | H8A–C8–H8B | 109.5 | C4–C3–C2 | 120.8 (4) | H1A–C1–H1B | 107.8 | C3–C4–C5 | 121.0 (4) | H1C–N1–H1E | 109.5 | C4–C5–C6 | 117.9 (4) | H1D–N1–H1E | 109.5 | C4–C5–C8 | 121.2 (4) | H8B–C8–H8C | 109.5 | C6–C5–C8 | 120.9 (4) | H1C–N1–H1D | 109.5 | C7–C6–C5 | 120.5 (4) | | |
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Symmetry codes: (i) x, −y + 1/2, z; (ii) x, y, z − 1; (iii) x − 1/2, y, −z + 1/2; (iv) x, y, z + 1; (v) x + 1/2, y, −z + 1/2.
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