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LC-MS run | Fractionation method | LC method | MS method |
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2 h LC HCD 1 | No | 5–30% ACN over 90 minutes | Standard |
2 h LC HCD exclusion list | No | 5–30% ACN over 90 minutes | Exclusion list |
2 h LC HCD 2 | No | 5–30% ACN over 90 minutes | Standard |
2 h LC HCD 3 | No | 5–30% ACN over 90 minutes | Standard |
2 h LC HCD 4 | No | 5–30% ACN over 90 minutes | Standard |
2 h LC HCD 5 | No | 5–30% ACN over 90 minutes | Standard |
2 h LC HCD (m/z 300–1500) 1 | No | 5–30% ACN over 90 minutes | m/z 300–1500 |
2 h LC HCD (m/z 300–1500) 2 | No | 5–30% ACN over 90 minutes | m/z 300–1501 |
2 h LC HCD (m/z 300–1500) 3 | No | 5–30% ACN over 90 minutes | m/z 300–1502 |
2 h LC HCD (m/z 300–1500) 4 | No | 5–30% ACN over 90 minutes | m/z 300–1503 |
2 h LC HCD (m/z 300–536) | No | 5–30% ACN over 90 minutes | m/z 300–536 |
2 h LC HCD (m/z 531–679) | No | 5–30% ACN over 90 minutes | m/z 531–679 |
2 h LC HCD (m/z 674–840) | No | 5–30% ACN over 90 minutes | m/z 674–840 |
2 h LC HCD (m/z 835–1500) | No | 5–30% ACN over 90 minutes | m/z 835–1500 |
4 h LC HCD 1 | No | 5–30% ACN over 215 minutes | Standard |
4 h LC HCD 2 | No | 5–30% ACN over 215 minutes | Standard |
6 h LC HCD 1 | No | 5–30% ACN over 335 minutes | Standard |
6 h LC HCD 2 | No | 5–30% ACN over 335 minutes | Standard |
8 h LC HCD 1 | No | 5–30% ACN over 455 minutes | Standard |
8 h LC HCD 2 | No | 5–30% ACN over 455 minutes | Standard |
SCX fraction 1 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 2 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 3 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 4 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 5 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 6 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 7 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 8 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 9 2 h LC HCD | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 1 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 2 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 3 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 4 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 5 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 6 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 7 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 8 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 9 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 10 2 h LC HCD exclusion list | SCX chromatography | 5–30% ACN over 90 minutes | Exclusion list |
SCX fraction 1 2 h LC (15–30% ACN)-optimized LC gradient | SCX chromatography | 15–30% ACN over 90 minutes | Standard |
SCX fraction 2 2 h LC (15–30% ACN)-optimized LC gradient | SCX chromatography | 15–30% ACN over 90 minutes | Standard |
SCX fraction 3 2 h LC (5–30% ACN)-optimized LC gradient | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 4 2 h LC (0–30% ACN)-optimized LC gradient | SCX chromatography | 0–30% ACN over 90 minutes | Standard |
SCX fraction 5 2 h LC (0–30% ACN)-optimized LC gradient | SCX chromatography | 0–30% ACN over 90 minutes | Standard |
SCX fraction 6 2 h LC (5–30% ACN)-optimized LC gradient | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 7 2 h LC (10–30% ACN)-optimized LC gradient | SCX chromatography | 10–30% ACN over 90 minutes | Standard |
SCX fraction 8 2 h LC (5–30% ACN)-optimized LC gradient | SCX chromatography | 5–30% ACN over 90 minutes | Standard |
SCX fraction 9 2 h LC (0–30% ACN)-optimized LC gradient | SCX chromatography | 0–30% ACN over 90 minutes | Standard |
SCX fraction 10 4 h LC (5–30% ACN)-optimized LC gradient | SCX chromatography | 5–30% ACN over 215 minutes | Standard |
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