| Matrix | Analyte | LODs (ng/mL) | LOQs (ng/mL) | Linear range (ng/ML) | Linear equation | Related coefficient () | Spiked concentration (ng/mL) | Recovery (%) | RSD (%) | Matrix effect (%) |
| Blood | Xylazine | 0.3 | 1.0 | 2/2000 | = 2.37 × 103 + 3.15 × 102 | 0.9992 | 5, 50, 500 | 101.2, 107.4, 112.5 | 6.5, 6.1, 4.7 | 103.1, 105.3, 102.7 | DMA | 0.3 | 1.0 | 2/2000 | = 2.19 × 103 + 4.87 × 102 | 0.9981 | 5, 50, 500 | 95.1, 97.9, 102.7 | 8.6, 8.1, 7.2 | 105.7, 107.7, 104.2 |
| Urine | Xylazine | 0.2 | 0.6 | 2/2000 | = 2.75 × 103 + 5.16 × 102 | 0.9993 | 5, 50, 500 | 96.9, 110.5, 117.4 | 6.2, 4.8, 4.3 | 105.9, 102.6, 101.1 | DMA | 0.2 | 0.6 | 2/2000 | = 2.24 × 103 + 4.17 × 102 | 0.9984 | 5, 50, 500 | 93.8, 96.7, 101.7 | 8.1, 7.1, 6.8 | 108.2, 107.3, 102.7 |
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