International Journal of Polymer Science / 2016 / Article / Tab 1

Research Article

Synthesis of Poly(styrene-acrylates-acrylic acid) Microspheres and Their Chemical Composition towards Colloidal Crystal Films

Table 1

Summary data for microspheres prepared.

EntrySample IDComonomerMolar ratio
Sty : comonomer : AA
SDBS (mg) (nm)PDI(nm) (mV)Molar ratio
Sty : comonomer : AA

1Rx-24IOA79 : 10 : 111.582800.024255−53.577 : 18 : 5
2Rx-4177 : 12 : 110.793200.020−50.473 : 22 : 5
3Rx-421.582550.088−56.473 : 23 : 4
4Rx-6670 : 20 : 100.792300.032−49.755 : 39 : 6
5Rx-671.582750.049−32.154 : 39 : 7
6Rx-49EHA81 : 13 : 060.792710.023−39.565 : 16 : 19
7Rx-3079 : 10 : 110.792860.043256−45.569 : 22 : 9
8Rx-291.582500.073−49.567 : 21 : 13
9Rx-7270 : 20 : 100.792600.057−52.468 : 25 : 7
10Rx-731.582390.037−55.462 : 32 : 6
11Rx-26IBA79 : 10 : 1102380.066−43.476 : 15 : 9
12Rx-270.792730.038−44.776 : 13 : 11
13Rx-4377 : 12 : 1202610.031204−51.670 : 19 : 11
14Rx-440.793040.066−50.067 : 25 : 8
15Rx-451.582280.022−52.469 : 18 : 13
16RX-5381 : 13 : 060.792860.028276−43.578 : 18 : 4
17Rx-37HA79 : 10 : 111.582700.047248−50.375 : 18 : 7
18Rx-5677 : 12 : 110.792600.038−44.974 : 21 : 5
19Rx-571.582770.010−44.671 : 21 : 8
20Rx-6968 : 22 : 101.582520.115−25.765 : 30 : 5
21Rx-33BA79 : 10 : 110.793320.070−50.566 : 17 : 17
22Rx-351.582790.025−43.270 : 20 : 10
23Rx-6177 : 12 : 110.792550.054−37.368 : 18 : 14
24Rx-621.582120.061−43.273 : 16 : 11

Molar ratio of monomers in the feed.
Determined by DLS.
PDI polydispersity by DLS.
Determined by TEM.
zeta potential.
Molar ratios of polymers in the microsphere by 1H-NMR.

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