Research Article
Two New Cytotoxic Candidaspongiolides from an Indonesian Sponge
Table 1
13C NMR data for compounds 1, 2, and 3.
| C no. | | | | |
| 1 | 171.3 qC | 171.3 qC | 171.3 qC | 171.3 qC | 2 | 70.7 CH | 70.8 CH | 70.8 CH | 72.9 CH | 3 | 83.4 CH | 83.3 CH | 83.1 CH | 84.7 CH | 4 | 47.8 CH | 47.7 CH | 47.9 CH | 49.5 CH | 5 | 214.6 qC | 214.9 qC | 216.2 qC | 217.6 qC | 6 | 48.5 CH | 48.3 CH | 49.8 CH | 51.1 CH | 7 | 80.1 CH | 80.1 CH | 79.2 CH | 79.9 CH | 8 | 131.6 qC | 132.0 qC | 136.2 qC | 139.0 qC | 9 | 132.0 CH | 131.7 CH | 129.4 CH | 129.8 CH | 10 | 46.2 CH | 46.1 CH | 45.9 CH | 46.5 CH | 11 | 211.5 qC | 211.7 qC | 211.9 qC | 212.7 qC | 12 | 42.6 CH2 | 42.7 CH2 | 42.5 CH2 | 44.3 CH2 | 13 | 68.9 CH | 68.8 CH | 69.0 CH | 69.3 CH | 14 | 81.6 qC | 81.6 qC | 81.6 qC | 85.0 qC | 15 | 210.8 qC | 211.0 qC | 211.2 qC | 216.5 qC | 16 | 46.9 CH | 47.0 CH | 46.9 CH | 46.4 CH | 17 | 77.8 CH | 77.7 CH | 77.7 CH | 78.4 CH | 18 | 62.7 qC | 62.7 qC | 62.6 qC | 63.9 qC | 19 | 67.1 CH | 67.0 CH | 67.0 CH | 67.4CH | 20 | 31.1 CH | 31.1 CH | 30.9 CH | 32.4 CH | 21 | 129.7 CH | 129.4 CH | 129.6 CH | 131.6 CH | 22 | 125.5 CH | 125.5 CH | 125.4 CH | 126.2 CH | 23 | 13.5 CH3 | 13.4 CH3 | 13.3 CH3 | 13.3 CH3 | 24 | 14.6 CH3 | 14.5 CH3 | 14.4 CH3 | 15.3 CH3 | 25 | 14.7 CH3 | 14.5 CH3 | 15.0 CH3 | 15.6 CH3 | 26 | 10.8 CH3 | 10.7 CH3 | 10.2 CH3 | 10.5 CH3 | 27 | 16.3 CH3 | 16.2 CH3 | 16.4 CH3 | 15.7 CH3 | 28 | 63.5 CH2 | 63.5 CH2 | 63.5 CH2 | 65.7 CH2 | 29 | 63.2 CH2 | 63.2 CH2 | 62.8 CH2 | 64.8 CH2 | 30 | 11.1 CH3 | 11.0 CH3 | 10.9 CH3 | 11.5 CH3 | 31 | 18.6 CH3 | 18.4 CH3 | 18.3 CH3 | 18.7 CH3 | 32 | 60.3 CH3 | 60.3 CH3 | 60.3 CH3 | 60.3 CH3 | 33 | 169.5 qC | 169.9 qC | — | — | 34 | 21.6 CH3 | 21.5 CH3 | — | — | 35 | 173.5 qC | 173.7 qC | 173.6 qC | — | 36 | 34.2 CH2 | 34.1 CH2 | 34.0 CH2 | — | 37 | 29.0 CH2 | 29.0 CH2 | 29.1 CH2 | — |
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easured in CDCl3. easured in CD3OD.
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