Research Article

ZSM-5-SO3H: An Efficient Catalyst for Acylation of Sulfonamides Amines, Alcohols, and Phenols under Solvent-Free Conditions

Table 3

ZSM-5-SO3H catalyzed acylation of alcohols and phenols under solvent-free conditions.

EntryAlcohol (phenol)Acylating agentProductsTime, min.
(yield, %)

1951749.table.003-1a951749.table.003-1b951749.table.003-1c10 (80)
2951749.table.003-2a951749.table.003-2b951749.table.003-2c15 (81)
3951749.table.003-3a951749.table.003-3b951749.table.003-3c15 (83)
4951749.table.003-4a951749.table.003-4b951749.table.003-4c25 (70)
5951749.table.003-5a951749.table.003-5b951749.table.003-5c10 (90)
15 (89)a
6951749.table.003-6a951749.table.003-6b951749.table.003-6c10 (89)
7951749.table.003-7a951749.table.003-7b951749.table.003-7c10 (88)
8951749.table.003-8a951749.table.003-8b951749.table.003-8c5 (95)
9951749.table.003-9a951749.table.003-9b951749.table.003-9c3 (95)
10951749.table.003-10a951749.table.003-10b951749.table.003-10c5 (93)
11951749.table.003-11a951749.table.003-11b951749.table.003-11c5 (95)
12951749.table.003-12a951749.table.003-12b951749.table.003-12c5 (95)
13951749.table.003-13a951749.table.003-13b951749.table.003-13c5 (96)
14951749.table.003-14a951749.table.003-14b951749.table.003-14c5 (75)
15951749.table.003-15a951749.table.003-15b951749.table.003-15c5 (81)
16951749.table.003-16a951749.table.003-16b951749.table.003-16c3 (88)
17951749.table.003-17a951749.table.003-17b951749.table.003-17c4 (85)
18951749.table.003-18a951749.table.003-18b951749.table.003-18c4 (80)
6 (75)a
19951749.table.003-19a951749.table.003-19b951749.table.003-19c5 (75)
20951749.table.003-20a951749.table.003-20b951749.table.003-20c5 (68)
21951749.table.003-21a951749.table.003-21b951749.table.003-21c5 (61)
22951749.table.003-22a951749.table.003-22b951749.table.003-22c2 (75)
23951749.table.003-23a951749.table.003-23b951749.table.003-23c3 (69)
24951749.table.003-24a951749.table.003-24b951749.table.003-24c3 (61)
25951749.table.003-25a951749.table.003-25b951749.table.003-25c1 (80)
26951749.table.003-26a951749.table.003-26b951749.table.003-26c2 (75)
27951749.table.003-27a951749.table.003-27b951749.table.003-27c2 (60)
28951749.table.003-28a951749.table.003-28b951749.table.003-28c2 (82)
29951749.table.003-29a951749.table.003-29b951749.table.003-29c2 (85)
30951749.table.003-30a951749.table.003-30b951749.table.003-30c2 (80)
31951749.table.003-31a951749.table.003-31b951749.table.003-31c5 (84)
32951749.table.003-32a951749.table.003-32b951749.table.003-32c1 (68)
33951749.table.003-33a951749.table.003-33b951749.table.003-33c1 (70)
34951749.table.003-34a951749.table.003-34b951749.table.003-34c1 (74)
35951749.table.003-35a951749.table.003-35b951749.table.003-35c5 (33)
36951749.table.003-36a951749.table.003-36b951749.table.003-36c5 (43)
37951749.table.003-37a951749.table.003-37b951749.table.003-37c5 (70)
38951749.table.003-38a951749.table.003-38b951749.table.003-38c5 (75)

20 mmol scale.