To robotize chemistry laboratories. An example of organic synthesis: 2-Boc-amino-<i>N</i>-hydroxy-3-phenyl-propionamide

Christophe, G.; Chapelant, L.; Bostyn, S.; Porte, C.; Delacroix, A.; D'Orchymont, H.

doi:https://doi.org/10.1155/S1463924602000032

Journal of Analytical Methods in Chemistry

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Volume 24 | Article ID 147546 | https://doi.org/10.1155/S1463924602000032

To robotize chemistry laboratories. An example of organic synthesis: 2-Boc-amino-N-hydroxy-3-phenyl-propionamide

G. Christophe,¹L. Chapelant,¹S. Bostyn,¹C. Porte,¹A. Delacroix,¹and H. D'Orchymont²

Abstract

The paper describes the development of periodic modules used for the peptide synthesis of hydroxamic acid. A powder conveyor using the principle of positive weighing distribution is described. Purification is provided using automatic filtration and a liquid—liquid extraction module separation device. Device quality is improved using failure mode and effects analysis.

Copyright

Copyright © 2002 Hindawi Publishing Corporation. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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