Research Article

Response Surface Optimization of a Rapid Ultrasound-Assisted Extraction Method for Simultaneous Determination of Tetracycline Antibiotics in Manure

Table 4

Figures of merit for TCs using the proposed UAE.

TCsLinear regression equationLOD g/mLLOQ g/mLMQL mg/kgRecovery%RSD%

OTC0.9966500.030.101.7592.422.94
TC0.9969600.030.101.9587.853.88
CTC0.9965590.050.172.3281.894.06
DC0.9932160.030.102.1584.462.37

Recoveries and RSD were obtained at the concentration of 50 g/g.