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Journal of Analytical Methods in Chemistry
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Journal of Analytical Methods in Chemistry
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2015
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Article
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Tab 2
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Research Article
Development of a Method to Detect Three Monohydroxylated Polycyclic Aromatic Hydrocarbons in Human Urine by Liquid Chromatographic Tandem Mass Spectrometry
Table 2
Recovery and precision data for 1-OHP, 3-OHBaP, and 3-OHBaA.
ć
Spiked
Conc.
Recovery
Intraday precision
Interday precision
ng/mL
ng/mL
, (%)
, (%)
, (%)
1-OHP
0.015
0.016
106.7
6.5
11.4
0.076
0.080
105.6
5.1
4
0.23
0.24
104.3
5.5
4
3-OHBaP
0.003
0.002
72.1
8.8
5.9
0.015
0.012
80.2
4.5
7.3
0.045
0.036
80.7
5.2
6
3-OHBaA
0.008
0.007
87.5
6.1
8.4
0.038
0.036
94.7
5.8
6.7
0.114
0.1135
99.6
3.9
1.8