Research Article
Determining the Levels of Four Phenylethanoid Glycosides and Five Triterpene Acids in Liuwei Dihuang Capsule Using Solid Phase Extraction with HPLC-UV
Table 3
Determination of the four phenylethanoid glycosides and five triterpene acids in 18 batches of LDC samples from six manufacturers (n = 3).
| Sample | Content (μg/capsule) | Purpureaside C | Jionoside A1 | Acteoside | Isoacteoside | Total phenlyethanoid glycosides | 3-O-Acetyl-16α-hydroxytrametenolic acid | Dehydropachymic acid | Pachymic acid | Trametenolic acid | Dehydrotrametenolic acid | Total triterpene acids |
| LDC01 | 10.8 | 14.3 | 18.2 | 8.1 | 51.4 | 3.0 | 13.0 | 82.6 | 13.2 | 4.0 | 115.8 | LDC02 | 10.2 | 16.4 | 20.1 | 8.9 | 55.6 | 3.0 | 12.7 | 74.8 | 11.3 | 3.8 | 105.6 | LDC03 | 12.0 | 15.3 | 19.5 | 8.6 | 55.4 | 3.2 | 12.2 | 57.2 | 14.4 | 3.6 | 90.6 | LDC04 | 8.3 | 10.5 | 17.8 | 7.4 | 44.0 | 4.5 | 20.1 | 72.2 | 29 | 23.2 | 149 | LDC05 | 8.8 | 11.4 | 18.3 | 7.5 | 46.0 | 4.1 | 20.7 | 65.0 | 22.3 | 20.9 | 133 | LDC06 | 9.7 | 11.9 | 18.8 | 8.2 | 48.6 | 3.4 | 20.2 | 63.6 | 21.8 | 20.1 | 129.9 | LDC07 | 13.2 | 15.6 | 23.4 | 10.1 | 62.3 | 1.8 | 27.7 | 75.8 | 16.4 | 11.3 | 133.0 | LDC08 | 12.6 | 14.7 | 22.8 | 9.8 | 59.9 | 1.8 | 27.6 | 74.6 | 15.6 | 10.8 | 130.5 | LDC09 | 14.1 | 16.9 | 24.5 | 9.7 | 65.2 | 1.9 | 27.7 | 74.7 | 16.9 | 11.8 | 132.9 | LDC10 | 13.6 | 13.7 | 25.1 | 9.2 | 61.6 | 1.6 | 34.0 | 58.5 | 29.9 | 13.9 | 137.9 | LDC11 | 12.8 | 13.1 | 24.8 | 9.4 | 60.1 | 1.6 | 33.4 | 58.1 | 28.7 | 13.7 | 135.4 | LDC12 | 11.3 | 14.1 | 25.9 | 8.7 | 60.0 | 1.6 | 33.6 | 57.0 | 30.6 | 13.7 | 136.5 | LDC13 | 10.7 | 13.7 | 20.5 | 8.5 | 53.4 | 1.4 | 11.2 | 44.6 | 6.1 | 5.5 | 68.7 | LDC14 | 11.5 | 12.4 | 23.1 | 8.9 | 55.9 | 1.3 | 11.7 | 46.5 | 6.5 | 5.4 | 71.5 | LDC15 | 9.7 | 10.1 | 19.3 | 7.8 | 46.9 | 1.4 | 10.8 | 45.1 | 6.0 | 5.9 | 69.3 | LDC16 | 8.4 | 9.2 | 16.5 | 6.9 | 41.0 | 3.4 | 19.0 | 53.5 | 23.0 | 17.7 | 116.5 | LDC17 | 7.9 | 8.6 | 16.9 | 6.2 | 39.6 | 3.0 | 18.6 | 50.1 | 22.1 | 19.8 | 113.6 | LDC18 | 9.8 | 9.3 | 18.8 | 9.1 | 47.0 | 3.5 | 18.5 | 54.5 | 23.0 | 17.3 | 116.8 |
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